methyl (2Z)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-deoxy-2-phenyl-D-manno-oct-2-enonate

Base Information

Chemical Name:methyl (2Z)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-deoxy-2-phenyl-D-manno-oct-2-enonate
CAS No.:1360590-02-8
Molecular Formula:C₂₁H₂₆O₇
Molecular Weight:390.433
Hs Code.:

Synonyms:methyl (2Z)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-deoxy-2-phenyl-D-manno-oct-2-enonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2Z)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-deoxy-2-phenyl-D-manno-oct-2-enonate

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Technology Process of methyl (2Z)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-deoxy-2-phenyl-D-manno-oct-2-enonate

There total 1 articles about methyl (2Z)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-deoxy-2-phenyl-D-manno-oct-2-enonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1360589-95-2
methyl (2E)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-bromo-2-deoxy-D-manno-oct-2-enonate

: 98-80-6
phenylboronic acid

: 1360590-02-8
methyl (2Z)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-deoxy-2-phenyl-D-manno-oct-2-enonate

Guidance literature:: methyl (2E)-3,7-anhydro-4,5:6,8-bis-O-(1-methylethylidene)-2-bromo-2-deoxy-D-manno-oct-2-enonate; phenylboronic acid; With potassium carbonate; In 1,4-dioxane; water; for 0.166667h;

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 110 ℃; for 24h;
DOI:10.1002/ejoc.201100949