C₄₇H₅₁N₃Si

Base Information

Chemical Name:C₄₇H₅₁N₃Si
CAS No.:174753-27-6
Molecular Formula:C₄₇H₅₁N₃Si
Molecular Weight:686.028
Hs Code.:

C<sub>47</sub>H<sub>51</sub>N<sub>3</sub>Si

Synonyms:C₄₇H₅₁N₃Si

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Chemical Property of C₄₇H₅₁N₃Si

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Technology Process of C₄₇H₅₁N₃Si

There total 14 articles about C₄₇H₅₁N₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 174753-25-4
[2-Ethyl-4-(2-ethyl-4-iodo-phenylethynyl)-phenylethynyl]-trimethyl-silane

: 174753-26-5
C₂₄H₂₇N₃

: 174753-27-6
C₄₇H₅₁N₃Si

Guidance literature:: With copper(l) iodide; diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; for 120h;
DOI:10.1021/jo962336q

Reference yield:

: 121-89-1
3-Nitroacetophenone

: 174753-27-6
C₄₇H₅₁N₃Si

Guidance literature:: Multi-step reaction with 11 steps

1: 12.29 g / conc. HCl, H₂ / Pd/C / ethanol / 70 °C / 3102.9 Torr

2: 96 percent / 1 M NaOH / tetrahydrofuran / 2 h / Heating

3: AlCl₃ / CS₂ / 70 °C

4: 3 M KOH

5: aq. HCl, NaNO₂ / 0.5 h / 0 °C

6: K₂CO₃ / 0.5 h / 0 °C

8: 99 percent / MeI / 120 °C

9: 90 percent / Pd(dba)2, Ph₃P, CuI, i-Pr₂NH / tetrahydrofuran / 24 h

10: 96 percent / MeI / 120 °C

11: 93 percent / Pd(dba)2, Ph₃P, CuI, i-Pr₂NH / tetrahydrofuran / 120 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; copper(l) iodide; aluminium trichloride; hydrogen; potassium carbonate; diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium nitrite; methyl iodide; palladium on activated charcoal; In tetrahydrofuran; carbon disulfide; ethanol;
DOI:10.1021/jo962336q

Reference yield:

: 187867-45-4
4-(diethyltriazenyl)-2-ethylacetophenone

: 174753-27-6
C₄₇H₅₁N₃Si

Guidance literature:: Multi-step reaction with 5 steps

2: 99 percent / MeI / 120 °C

3: 90 percent / Pd(dba)2, Ph₃P, CuI, i-Pr₂NH / tetrahydrofuran / 24 h

4: 96 percent / MeI / 120 °C

5: 93 percent / Pd(dba)2, Ph₃P, CuI, i-Pr₂NH / tetrahydrofuran / 120 h

With copper(l) iodide; diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; methyl iodide; In tetrahydrofuran;
DOI:10.1021/jo962336q