bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium

Base Information

Chemical Name:bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium
CAS No.:1307795-15-8
Molecular Formula:C₁₆H₂₅BrF₂MgOSi
Molecular Weight:403.665
Hs Code.:

Synonyms:bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium

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Chemical Property of bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium

Chemical Property:

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Technology Process of bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium

There total 3 articles about bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1307795-17-0
[(2-bromo-4,5-difluorobenzyl)oxy](triisopropyl)silane

: 7439-95-4
magnesium

: 1307795-15-8
bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium

Guidance literature:: In tetrahydrofuran; at 20 - 45 ℃; for 3h;

Reference yield:

: 64695-84-7
2-bromo-4,5-difluorobenzoic acid

: 1307795-15-8
bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / Reflux

2: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C

3: tetrahydrofuran / 3 h / 20 - 45 °C

With 1H-imidazole; dimethylsulfide borane complex; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 476620-55-0
(2-bromo-4,5-difluorophenyl)methanol

: 1307795-15-8
bromo(4,5-difluoro-2-{[(triisopropylsilyl)oxy]methyl}phenyl)magnesium

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C

2: tetrahydrofuran / 3 h / 20 - 45 °C

With 1H-imidazole; In tetrahydrofuran; N,N-dimethyl-formamide;