2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole

Base Information

• Chemical Name: 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole
• CAS No.: 271788-60-4
• Molecular Formula: C₂₁H₂₆ClN₃O
• Molecular Weight: 371.91

Synonyms:2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole

Chemical Property of 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole

Chemical Property:

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Technology Process of 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole

There total 3 articles about 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

(5-chloro-2-nitro-phenyl)-(3,5-di-tert-butyl-2-methoxy-phenyl)-diazene → 3,5-di-tert-butyl-2-methoxyaniline (893397-17-6) + 4-Chloro-1,2-phenylenediamine (95-83-0) + 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole (271788-60-4) + 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-1-oxido-2H-benzotriazole

Guidance literature:

With lithium perchlorate; In methanol; dichloromethane; at 20 ℃; Electrolysis;

DOI:10.3987/com-99-8824

Reference yield: 63.0%

(5-chloro-2-nitro-phenyl)-(3,5-di-tert-butyl-2-methoxy-phenyl)-diazene → 3,5-di-tert-butyl-2-methoxyaniline (893397-17-6) + 4-Chloro-1,2-phenylenediamine (95-83-0) + 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole (271788-60-4)

Guidance literature:

With sodium hydroxide; lithium perchlorate; In tetrahydrofuran; water; at 20 ℃; Electrolysis;

DOI:10.3987/com-99-8824

Reference yield: 60.0%

(4-chloro-2-nitro-phenyl)-(3,5-di-tert-butyl-2-methoxy-phenyl)-diazene → 3,5-di-tert-butyl-2-methoxyaniline (893397-17-6) + 4-Chloro-1,2-phenylenediamine (95-83-0) + 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-5-chloro-2H-benzotriazole (271788-60-4) + 2-[3,5-bis(1,1-dimethylethyl)-2-methoxyphenyl]-6-chloro-1-oxido-2H-benzotriazole

Guidance literature:

With lithium perchlorate; In methanol; dichloromethane; at 20 ℃; Electrolysis;

DOI:10.3987/com-99-8824

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