2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester

Base Information

Chemical Name:2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester
CAS No.:1448711-33-8
Molecular Formula:C₂₁H₂₈O₅
Molecular Weight:360.45
Hs Code.:

Synonyms:2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester

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Chemical Property of 2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester

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Technology Process of 2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester

There total 3 articles about 2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1448711-32-7
2,4-dimethoxy-6-methyl-benzoic acid1-methyl-hex-5-enyl ester

: 109480-79-7,121712-52-5
(E)-N-methoxy-N-methyl-2-butenamide

: 1448711-33-8
2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester

Guidance literature:: 2,4-dimethoxy-6-methyl-benzoic acid1-methyl-hex-5-enyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.25h;

(E)-N-methoxy-N-methyl-2-butenamide; In tetrahydrofuran; for 1h;
DOI:10.1002/cjoc.201300016

Reference yield:

: 1276019-92-1
C₁₄H₂₀O₄

: 1448711-33-8
2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol; water / 12 h / Reflux

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / -78 °C

3.2: 1 h

With triphenylphosphine; potassium hydroxide; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; ethanol; water; 2.1: |Mitsunobu Displacement;
DOI:10.1002/cjoc.201300016

Reference yield:

: 3686-57-5
2,4-dimethoxy-6-methylbenzoic acid

: 1448711-33-8
2,4-dimethoxy-6-(2-oxo-pent-3-enyl)-benzoic acid 1-methyl-hex-5-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / -78 °C

2.2: 1 h

With triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; 1.1: |Mitsunobu Displacement;
DOI:10.1002/cjoc.201300016