tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane

Base Information

Chemical Name:tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane
CAS No.:187843-63-6
Molecular Formula:C₂₇H₃₂O₂SeSi
Molecular Weight:495.595
Hs Code.:

Synonyms:tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane

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Technology Process of tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane

There total 1 articles about tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 645-96-5
Benzeneselenol

: methyl 5-O-(tert-butyldiphenylsilyl)-2,3-dideoxy-α,β-D-glycero-pentofuranoside

: 187843-63-6
tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane

: 187843-66-9
tert-Butyl-diphenyl-((2S,5S)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane

Guidance literature:: With boron trifluoride diethyl etherate; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, -10 deg C, 10 min, 2.) -20 deg C, 45 min;
DOI:10.1021/jo9616825

Reference yield: 63.0%

: 187843-63-6
tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane

: 149204-36-4
(1S)-1-<<(tert-butyldiphenylsilyl)oxy>methyl>-2,3-dihydrofuran

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene;
DOI:10.1021/jo9616825

Reference yield:

: 187843-63-6
tert-Butyl-diphenyl-((2S,5R)-5-phenylselanyl-tetrahydro-furan-2-ylmethoxy)-silane

: 141684-79-9
1-<5-O-(tert-butyldiphenylsilyl)-3-deoxy-2-Se-phenyl-2-seleno-β-D-erythro-pentofuranosyl>uracil

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / EtiPr₂N, tBuOOH, Ti(OiPr)4 / CH₂Cl₂; toluene

2: AgOTf / diethyl ether / 1 h / Ambient temperature

With titanium(IV) isopropylate; tert.-butylhydroperoxide; silver trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo9616825