N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

Base Information

Chemical Name:N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine
CAS No.:1275581-91-3
Molecular Formula:C₂₁H₂₆ClN₅O₃
Molecular Weight:431.922
Hs Code.:

Synonyms:N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

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Chemical Property of N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

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Technology Process of N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

There total 4 articles about N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 110-91-8,99108-56-2
morpholine

: 1275581-90-2
N-(1,3-benzodioxol-5-ylmethyl)-4,6-dichloro-N-cyclohexyl-1,3,5-triazin-2-amine

: 1275581-91-3
N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 25 ℃; for 21h; Inert atmosphere;
DOI:10.1039/c2ob00034b

Reference yield:

: 227017-79-0
N-(1,3-benzodioxol-5-ylmethyl)cyclohexanamine

: 1275581-91-3
N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 21 h / 0 - 25 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/c2ob00034b

Reference yield:

: 2620-50-0
1,3-benzodioxol-5-ylmethyl amine

: 1275581-91-3
N-(1,3-benzodioxol-5-ylmethyl)-4-chloro-N-cyclohexyl-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 1.5 h / 25 °C / Molecular sieve; Inert atmosphere

1.2: 25 h / 17 °C / Molecular sieve; Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 21 h / 0 - 25 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/c2ob00034b