Technology Process of C43H64O6S
There total 8 articles about C43H64O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane;
at -20 ℃;
for 3h;
DOI:10.1246/bcsj.62.2599
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 67 percent / pyridinium p-toluenesulfonate / CH2Cl2 / 4 h / Ambient temperature
2: 77 percent / lithium bromide, lithium carbonate / dimethylformamide / 1 h / 70 °C
3: BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 3 h / -20 °C
With
n-butyllithium; pyridinium p-toluenesulfonate; lithium carbonate; lithium bromide;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.62.2599
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 65 percent / NaH / dimethylsulfoxide; tetrahydrofuran / 3 h / 0 °C
2: 76 percent / pyridinium p-toluenesulfonate / CH2Cl2 / 6 h / Ambient temperature
3: BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 3 h / -20 °C
With
n-butyllithium; pyridinium p-toluenesulfonate; sodium hydride;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.1246/bcsj.62.2599