Dithiocarbonic acid O-methyl S-sodium salt

Base Information

• Chemical Name: Dithiocarbonic acid O-methyl S-sodium salt
• CAS No.: 6370-03-2
• Molecular Formula: C₂H₃OS₂*Na
• Molecular Weight: 130.167
• Mol file: 6370-03-2.mol

Synonyms:sodium methyl xanthate

Chemical Property of Dithiocarbonic acid O-methyl S-sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Dithiocarbonic acid O-methyl S-sodium salt

There total 1 articles about Dithiocarbonic acid O-methyl S-sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H18OS2Te → biphenyl (92-52-4,1594-86-1) + diphenyltellurium(IV) oxide (51786-98-2) + sodium methyl xanthate (6370-03-2)

Guidance literature:

With oxygen; In toluene; benzene; for 120h; Product distribution; Ambient temperature; Irradiation; Chloroform is also solvent; with or without O₂; further xanthates, dithiocarbamates and dithiophosphates;

DOI:10.1016/0022-328X(89)85332-X

Reference yield: 97.0%

cis-dichlorodioxobis(triphenylphosphine oxide)molybdenum(VI) + sodium methyl xanthate (6370-03-2) → (dioxomolybdenum)Cl(methyl xanthate)(triphenylphosphine oxide)

Guidance literature:

In dichloromethane; byproducts: OP(C6H5)3, NaCl; soln. of MoO2Cl2(OP(C6H5)3)2 in CH2Cl2 added with stirring at room temp.to susp. of Na(CH3OCS2)2 in CH2Cl2, mixt. stirring 3 h; NaCl fitered off, washed with CH2Cl2, filtrate concd., solid dried in vacuo and repeated washing with dried benzene; elem. anal.;

DOI:10.1081/SIM-120015079

Reference yield: 94.8%

sodium methyl xanthate (6370-03-2) + N-butylamine (109-73-9,85404-21-3) + phenylacetylene (536-74-3) → (2-phenylvinyl) N-n-butyldithiocarbamate

Guidance literature:

In ethylene glycol; at 80 ℃; for 1h;

Downstream raw materials:

Methyl xanthogenic acid benzylester

O-Methyl-S--xanthogenat

anti-S-(2-Hydroxyimino-2-phenylethyl) O-methyl dithiocarbonate

2-<(methoxythiocarbonylthio)acetyl>-5,5-dimethyl-1,3-cyclohexanedione