(Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid

Base Information

Chemical Name:(Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid
CAS No.:193468-18-7
Molecular Formula:C₁₃H₁₅NO₃
Molecular Weight:233.267
Hs Code.:

Synonyms:(Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid

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Chemical Property of (Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid

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Technology Process of (Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid

There total 4 articles about (Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: (Z)-3-[((Z)-3-Carboxy-but-2-enoyl)-((S)-1-phenyl-ethyl)-amino]-2-methyl-but-2-enoic acid ethyl ester

: 609-14-3
2-acetylpropanoic acid ethyl ester

: 193468-18-7
(Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid

Guidance literature:: With water; at 20 ℃; for 0.166667h;
DOI:10.1016/S0040-4039(97)01046-0

Reference yield:

: 193468-16-5,92701-94-5
(2Z)-(+)-ethyl 2-methyl-3-[(S)-α-methylbenzylamino]-2-butenoate

: 193468-18-7
(Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 5 h / Heating

2: water

With water; In tetrahydrofuran;
DOI:10.3987/COM-97-S(N)47

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 193468-18-7
(Z)(S)-N-(1'-phenylethyl)-2-methylmaleamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / tetrahydrofuran / 12 h / Heating

2: tetrahydrofuran / 5 h / Heating

3: 60 percent / H₂O / 0.17 h / 20 °C

With water; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)01046-0