(1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

Base Information

Chemical Name:(1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide
CAS No.:1357917-61-3
Molecular Formula:C₁₆H₁₉N₃O₃
Molecular Weight:301.345
Hs Code.:

Synonyms:(1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

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Technology Process of (1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

There total 6 articles about (1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 930-88-1
N-methylmaleimide

: 1357917-76-0
2-benzylideneamino-N,N-dimethylacetamide

: 1357917-61-3
(1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

Guidance literature:: With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; tetrakis(actonitrile)copper(I) hexafluorophosphate; triethylamine; In tetrahydrofuran; at 20 ℃; for 48h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c2cc17149j

Reference yield:

: 930-88-1
N-methylmaleimide

: 1357917-76-0
2-benzylideneamino-N,N-dimethylacetamide

: 1357917-61-3
(1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

: (1S,3R,3aR,6aS)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; triethylamine; (R)-segphos; In tetrahydrofuran; at 20 ℃; for 10h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c2cc17149j

Reference yield:

: 930-88-1
N-methylmaleimide

: 1357917-76-0
2-benzylideneamino-N,N-dimethylacetamide

: 1357917-61-3
(1R,3S,3aS,6aR)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

: (1S,3R,3aR,6aS)-5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

: 5-methyl-4,6-dioxo-3-phenyl-octahydropyrrolo[3,4-c]pyrrole-1-N,N-dimethylcarboxamide

Guidance literature:: With silver(I) acetate; triethylamine; (R)-segphos; In tetrahydrofuran; at 20 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c2cc17149j