((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

Base Information

Chemical Name:((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene
CAS No.:898831-70-4
Molecular Formula:C₃₄H₃₄N₆O₄
Molecular Weight:590.682
Hs Code.:

Synonyms:((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

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Chemical Property of ((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

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Technology Process of ((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

There total 5 articles about ((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methanesulfonic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-methanesulfonyloxy-cyclohexyl ester

: 898831-70-4
((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 110 ℃; for 12h;
DOI:10.1021/jo049521l

Reference yield:

: 24558-77-8
3,4,5,6-tetra-O-benzyl inositol

: 898831-70-4
((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 20 h / 20 °C

2: 3.78 g / NaN₃ / dimethylformamide / 12 h / 110 °C

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1021/jo049521l

Reference yield:

: 138258-55-6
(1S,2R,3R,4S)-1,2,3,4,tetrahydroxy-5-cyclohexene

: 898831-70-4
((1S,2R,3R,4S,5R,6S)-5,6-diazidocyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 16 h / 30 °C

2: tert.-butylhydroperoxide; osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 20 °C

3: pyridine / 16 h / 20 °C

4: sodium azide / N,N-dimethyl-formamide / 12 h / 85 °C

With pyridine; tert.-butylhydroperoxide; osmium(VIII) oxide; sodium azide; water; sodium hydride; 4-methylmorpholine N-oxide; In N,N-dimethyl-formamide; acetone; mineral oil; tert-butyl alcohol;
DOI:10.1021/ml200098j