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C30H31N3O6S

Base Information
  • Chemical Name:C30H31N3O6S
  • CAS No.:1616280-24-0
  • Molecular Formula:C30H31N3O6S
  • Molecular Weight:561.659
  • Hs Code.:
C<sub>30</sub>H<sub>31</sub>N<sub>3</sub>O<sub>6</sub>S

Synonyms:C30H31N3O6S

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Chemical Property of C30H31N3O6S
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Technology Process of C30H31N3O6S

There total 21 articles about C30H31N3O6S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 55 ℃; for 4h;
Guidance literature:
Multi-step reaction with 5 steps
1: nickel dichloride; sodium tetrahydroborate / methanol / 0.33 h / 0 °C
2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 50 °C
3: potassium carbonate / methanol; tetrahydrofuran / 1 h / 20 °C
4: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 55 °C
With bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; 2: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling;
Guidance literature:
Multi-step reaction with 8 steps
1.1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 90 °C
1.2: 16 h / 90 °C
2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C
2.2: 1 h / 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 120 °C
4.1: ammonium chloride; iron / methanol; tetrahydrofuran; water / 1 h / 100 °C
5.1: potassium iodide; potassium iodate; hydrogenchloride / methanol; water; 1,4-dioxane / 1.5 h / 50 °C / Inert atmosphere
6.1: pyridine / 0.75 h / 0 - 20 °C
7.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere
8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 55 °C
With pyridine; hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; potassium iodate; copper(l) iodide; tetrabutyl ammonium fluoride; iron; sodium hydride; potassium carbonate; ammonium chloride; triethylamine; triphenylphosphine; potassium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; 7.1: |Sonogashira Cross-Coupling;
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