Technology Process of C30H31N3O6S
There total 21 articles about C30H31N3O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 55 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: nickel dichloride; sodium tetrahydroborate / methanol / 0.33 h / 0 °C
2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 50 °C
3: potassium carbonate / methanol; tetrahydrofuran / 1 h / 20 °C
4: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 55 °C
With
bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; nickel dichloride;
In
tetrahydrofuran; methanol;
2: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 90 °C
1.2: 16 h / 90 °C
2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C
2.2: 1 h / 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 120 °C
4.1: ammonium chloride; iron / methanol; tetrahydrofuran; water / 1 h / 100 °C
5.1: potassium iodide; potassium iodate; hydrogenchloride / methanol; water; 1,4-dioxane / 1.5 h / 50 °C / Inert atmosphere
6.1: pyridine / 0.75 h / 0 - 20 °C
7.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere
8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 55 °C
With
pyridine; hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; potassium iodate; copper(l) iodide; tetrabutyl ammonium fluoride; iron; sodium hydride; potassium carbonate; ammonium chloride; triethylamine; triphenylphosphine; potassium iodide;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
7.1: |Sonogashira Cross-Coupling;