methyl 3-methyl-1-oxo-9-phenyl-1H-2-oxa-6-azaphenanthrene-10-carboxylate

Base Information

Chemical Name:methyl 3-methyl-1-oxo-9-phenyl-1H-2-oxa-6-azaphenanthrene-10-carboxylate
CAS No.:1201815-52-2
Molecular Formula:C₂₁H₁₅NO₄
Molecular Weight:345.354
Hs Code.:

Synonyms:methyl 3-methyl-1-oxo-9-phenyl-1H-2-oxa-6-azaphenanthrene-10-carboxylate

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Chemical Property of methyl 3-methyl-1-oxo-9-phenyl-1H-2-oxa-6-azaphenanthrene-10-carboxylate

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Technology Process of methyl 3-methyl-1-oxo-9-phenyl-1H-2-oxa-6-azaphenanthrene-10-carboxylate

There total 2 articles about methyl 3-methyl-1-oxo-9-phenyl-1H-2-oxa-6-azaphenanthrene-10-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: C₂₂H₂₁NO₆

: 1201815-52-2
methyl 3-methyl-1-oxo-9-phenyl-1H-2-oxa-6-azaphenanthrene-10-carboxylate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20 ℃; Reflux; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.08.019

Reference yield: 30.0%

: 1201815-44-2
phenyl-(3-trimethylsilylethynylpyridin-4-yl)methanone

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 20540-69-6
pentacarbonyl(methoxymethylcarbene)chromium⁽⁰⁾

: 1201815-52-2
methyl 3-methyl-1-oxo-9-phenyl-1H-2-oxa-6-azaphenanthrene-10-carboxylate

: C₂₂H₂₁NO₆

Guidance literature:: phenyl-(3-trimethylsilylethynylpyridin-4-yl)methanone; dimethyl cis-but-2-ene-1,4-dioate; pentacarbonyl(methoxymethylcarbene)chromium⁽⁰⁾; In tetrahydrofuran; for 13h; Reflux; Inert atmosphere;

With hydrogenchloride; In diethyl ether; water; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.08.019