3-benzyloxy-2-ethyl-2-methoxypropanenitrile

Base Information

Chemical Name:3-benzyloxy-2-ethyl-2-methoxypropanenitrile
CAS No.:253317-27-0
Molecular Formula:C₁₃H₁₇NO₂
Molecular Weight:219.283
Hs Code.:

Synonyms:3-benzyloxy-2-ethyl-2-methoxypropanenitrile

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Chemical Property of 3-benzyloxy-2-ethyl-2-methoxypropanenitrile

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Technology Process of 3-benzyloxy-2-ethyl-2-methoxypropanenitrile

There total 1 articles about 3-benzyloxy-2-ethyl-2-methoxypropanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 3587-60-8
Benzyloxymethyl chloride

: 253317-26-9
2-methoxybutanenitrile

: 253317-27-0
3-benzyloxy-2-ethyl-2-methoxypropanenitrile

Guidance literature:: 2-methoxybutanenitrile; With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

Benzyloxymethyl chloride; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1246/bcsj.72.2307

Reference yield: 92.0%

: 253317-27-0
3-benzyloxy-2-ethyl-2-methoxypropanenitrile

: 253317-28-1
2-benzyloxymethyl-2-methoxy-1-butanamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 5h;
DOI:10.1246/bcsj.72.2307

Reference yield:

: 253317-27-0
3-benzyloxy-2-ethyl-2-methoxypropanenitrile

: 253317-29-2
N-(2-benzyloxymethyl-2-methoxybutyl)formamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / LiAlH₄ / diethyl ether / 5 h / 0 - 20 °C

2: 89 percent / 6 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; 1: Reduction / 2: Substitution;
DOI:10.1246/bcsj.72.2307