N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide

Base Information

Chemical Name:N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide
CAS No.:1404479-59-9
Molecular Formula:C₁₄H₂₀BrNO₂S
Molecular Weight:346.288
Hs Code.:

Synonyms:N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide

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Chemical Property of N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide

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Technology Process of N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide

There total 3 articles about N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 98-58-8
4-bromobenzenesulfonyl chloride

: 141511-50-4
2,2-dimethyl-1-amino-5-hexene

: 1404479-59-9
N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c2cc36067e

Reference yield:

: 84173-95-5
2,2-dimethyl-5-hexenenitrile

: 1404479-59-9
N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 21 h / 0 °C / Reflux

2: triethylamine / dichloromethane / 0 - 20 °C

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1039/c2cc36067e

Reference yield:

: 53545-96-3
6-bromo-2,2-dimethylhexanenitrile

: 1404479-59-9
N-(2,2-dimethylhex-5-en-1-yl)-4-bromolbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / tetrahydrofuran / 7 h / 0 - 20 °C

2: lithium aluminium tetrahydride / diethyl ether / 21 h / 0 °C / Reflux

3: triethylamine / dichloromethane / 0 - 20 °C

With lithium aluminium tetrahydride; potassium tert-butylate; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1039/c2cc36067e