Technology Process of C23H26O9
There total 8 articles about C23H26O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
ethanol;
at 100 - 120 ℃;
for 24h;
Inert atmosphere;
Sealed tube;
DOI:10.1021/ja209205x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium diacetate; silver carbonate; Trimethylacetic acid / hexafluoropropan-2-ol / 24 h / 75 °C / Inert atmosphere
2: sodium hydroxide / ethanol / 24 h / 100 - 120 °C / Inert atmosphere; Sealed tube
With
palladium diacetate; silver carbonate; sodium hydroxide; Trimethylacetic acid;
In
hexafluoropropan-2-ol; ethanol;
DOI:10.1021/ja209205x
- Guidance literature:
-
Multi-step reaction with 7 steps
1: dichloromethane / 96 h / 15 °C / Photolysis; Inert atmosphere
2: 10 % platinum on carbon; hydrogen / dichloromethane
3: 1,2-dichloro-ethane / 3 h / 0 - 23 °C / Inert atmosphere
4: palladium diacetate; silver carbonate; Trimethylacetic acid / hexafluoropropan-2-ol / 36 h / 20 - 90 °C / Sealed tube; Inert atmosphere
5: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.05 h / -15 °C / Inert atmosphere
6: palladium diacetate; silver carbonate; Trimethylacetic acid / hexafluoropropan-2-ol / 24 h / 75 °C / Inert atmosphere
7: sodium hydroxide / ethanol / 24 h / 100 - 120 °C / Inert atmosphere; Sealed tube
With
10 % platinum on carbon; hydrogen; palladium diacetate; potassium hexamethylsilazane; 1,2-dichloro-ethane; silver carbonate; sodium hydroxide; Trimethylacetic acid;
In
tetrahydrofuran; hexafluoropropan-2-ol; ethanol; dichloromethane; toluene;
DOI:10.1021/ja209205x
