7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one

Base Information

• Chemical Name: 7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one
• CAS No.: 111015-10-2
• Molecular Formula: C₁₉H₂₄O₃
• Molecular Weight: 300.398

Synonyms:7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one

Chemical Property of 7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one

Chemical Property:

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Technology Process of 7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one

There total 4 articles about 7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-2β,3,3aβ,4β,7,7aβ-hexahydro-2,4-methano-1H-inden-1-one (114506-75-1) → 7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one (111015-10-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/jo00249a010

Reference yield:

2-ethylcyclopentane-1,3-dione (823-36-9) → 7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one (111015-10-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 73 percent / triton B / xylene / Heating

2: 28 percent / HCl gas / methanol / 4 h / Ambient temperature

3: 98 percent / H₂ / 10percent Pd-C / methanol

With hydrogenchloride; hydrogen; N-benzyl-trimethylammonium hydroxide; palladium on activated charcoal; In methanol; xylene;

DOI:10.1021/jo00249a010

Reference yield:

5-Methoxy-3-(4-methoxy-phenyl)-pent-1-en-3-ol (56475-35-5) → 7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-inden-1-one (111015-10-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 73 percent / triton B / xylene / Heating

2: 28 percent / HCl gas / methanol / 4 h / Ambient temperature

3: 98 percent / H₂ / 10percent Pd-C / methanol

With hydrogenchloride; hydrogen; N-benzyl-trimethylammonium hydroxide; palladium on activated charcoal; In methanol; xylene;

DOI:10.1021/jo00249a010

upstream raw materials:

7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-2β,3,3aβ,4β,7,7aβ-hexahydro-2,4-methano-1H-inden-1-one

2-ethylcyclopentane-1,3-dione

5-Methoxy-3-(4-methoxy-phenyl)-pent-1-en-3-ol

2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

Downstream raw materials:

7a-ethyl-5-(p-methoxyphenyl)-1-methyl-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-indene-1,3a-diol

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