4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid

Base Information

Chemical Name:4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid
CAS No.:118683-29-7
Molecular Formula:C₂₅H₂₄O₇
Molecular Weight:436.461
Hs Code.:

Synonyms:4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid

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Chemical Property of 4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid

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Technology Process of 4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid

There total 7 articles about 4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 118684-04-1
tert-butyl 4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoate

: 118683-29-7
4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 192h; Ambient temperature;

Reference yield:

: 89-86-1
4-hydroxysalicylic acid

: 118683-29-7
4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 27 percent / POCl₃ / o-xylene / 1.5 h / 100 °C

2: K₂CO₃ / acetone / 18 h / Heating

3: 1 h / 200 °C

4: H₂ / 5percent Pd/C / ethanol / 1 h / 1551.4 Torr / Ambient temperature

5: 29 percent / K₂CO₃ / acetone / 24 h / Heating

6: 37 percent / CF₃CO₂H / CH₂Cl₂ / 192 h / Ambient temperature

With hydrogen; potassium carbonate; trifluoroacetic acid; trichlorophosphate; palladium on activated charcoal; In ethanol; dichloromethane; o-xylene; acetone;

Reference yield:

: 16700-99-5
phenyl 2,4-dihydroxybenzoate

: 118683-29-7
4-<(4-carbophenoxy-3-hydroxy-2-propylphenoxy)methyl>-3-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / acetone / 18 h / Heating

2: 1 h / 200 °C

3: H₂ / 5percent Pd/C / ethanol / 1 h / 1551.4 Torr / Ambient temperature

4: 29 percent / K₂CO₃ / acetone / 24 h / Heating

5: 37 percent / CF₃CO₂H / CH₂Cl₂ / 192 h / Ambient temperature

With hydrogen; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetone;