N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester

Base Information

Chemical Name:N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester
CAS No.:1214275-54-3
Molecular Formula:C₅₀H₇₅N₅O₈S
Molecular Weight:906.24
Hs Code.:

N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester

Synonyms:N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester

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Chemical Property of N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester

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Technology Process of N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester

There total 1 articles about N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1214275-52-1
diethyl 2-((E)-3-(5-formyl-1-methyl-1H-imidazol-2-yl)allyl)-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl)malonate

: H-VFM-OMe

: 1214275-54-3
N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester

Guidance literature:: H-VFM-OMe; With triethylamine; In methanol; dichloromethane; at 20 ℃; for 0.166667h; Molecular sieve;

diethyl 2-((E)-3-(5-formyl-1-methyl-1H-imidazol-2-yl)allyl)-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl)malonate; In methanol; dichloromethane; at 20 ℃; for 6h;

With sodium cyanoborohydride; acetic acid; In methanol; dichloromethane; at 20 ℃; for 15h;
DOI:10.1016/j.bmc.2009.12.017

Reference yield: 100.0%

: 1214275-54-3
N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester

: 1214275-56-5
N-((2-((1E,6E,10e)-4-carboxy-4-(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine

Guidance literature:: N-((2-((1E,6E,10E)-4,4-bis(ethoxycarbonyl)-7,11,15-trimethylhexadeca-1,6,10,14-tetraen-1-yl)-1-methyl-1H-imidazol-5-yl)methyl)-L-valyl-L-phenylalanyl-L-methionine methyl ester; With water; lithium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 168h;

With hydrogenchloride; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmc.2009.12.017