14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol

Base Information

Chemical Name:14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol
CAS No.:1356140-43-6
Molecular Formula:C₈₂H₁₅₈O₃
Molecular Weight:1192.15
Hs Code.:

Synonyms:14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol

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Chemical Property of 14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol

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Technology Process of 14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol

There total 9 articles about 14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1356140-29-8
1-bromo-8-methyl-4-(4-methylpentyl)nonane

: diethyl 5-[2-(benzyloxy)ethyl]nonanedioate

: 1356140-43-6
14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol

Guidance literature:: 1-bromo-8-methyl-4-(4-methylpentyl)nonane; With iodine; magnesium; In diethyl ether; for 2h; Inert atmosphere; Reflux;

diethyl 5-[2-(benzyloxy)ethyl]nonanedioate; With ethylene dibromide; In diethyl ether; for 5h; Inert atmosphere; Reflux;
DOI:10.1002/asia.201100480

Reference yield:

: C₁₈H₃₀O₄

: 1356140-43-6
14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol

Guidance literature:: Multi-step reaction with 3 steps

1.1: Jones reagent / acetone

2.1: sulfuric acid / 12 h / Reflux

2.2: 6 h / 20 °C / 760.05 Torr

3.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

3.2: 5 h / Inert atmosphere; Reflux

With Jones reagent; sulfuric acid; iodine; magnesium; In diethyl ether; acetone; 1.1: Jones oxidation;
DOI:10.1002/asia.201100480

Reference yield:

: 1356140-28-7
8-methyl-4-(4-methylpentyl)nonan-1-ol

: 1356140-43-6
14-[2-(benzyloxy)ethyl]-2,26-dimethyl-6,22-bis(4-methylpentyl)-10,18-bis[8-methyl-4-(4-methylpentyl)nonyl]heptacosane-10,18-diol

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide; triphenylphosphine / dichloromethane / 12.5 h / -78 - 20 °C / Inert atmosphere; Darkness

2.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

2.2: 5 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; iodine; magnesium; triphenylphosphine; In diethyl ether; dichloromethane;
DOI:10.1002/asia.201100480