RhAu(C₅H₄NCH(P(C₆H₅)2)2)2⁽²⁺⁾*BF₄^(1-)*NO₃^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2](BF₄)(NO₃)

Base Information

• Chemical Name: RhAu(C₅H₄NCH(P(C₆H₅)2)2)2⁽²⁺⁾*BF₄^(1-)*NO₃^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2](BF₄)(NO₃)
• CAS No.: 95936-62-2
• Molecular Formula: BF₄*C₆₀H₅₀AuN₂P₄Rh*NO₃
• Molecular Weight: 1371.65

Synonyms:RhAu(C₅H₄NCH(P(C₆H₅)2)2)2⁽²⁺⁾*BF₄^(1-)*NO₃^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2](BF₄)(NO₃)

Chemical Property of RhAu(C₅H₄NCH(P(C₆H₅)2)2)2⁽²⁺⁾*BF₄^(1-)*NO₃^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2](BF₄)(NO₃)

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Technology Process of RhAu(C₅H₄NCH(P(C₆H₅)2)2)2⁽²⁺⁾*BF₄^(1-)*NO₃^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2](BF₄)(NO₃)

There total 1 articles about RhAu(C₅H₄NCH(P(C₆H₅)2)2)2⁽²⁺⁾*BF₄^(1-)*NO₃^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2](BF₄)(NO₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

triphenylphosphinegold(I) nitrate + [Rh(((C6H5)2P)2CHC5H4N)2](1+)*BF4(1-)=[Rh(((C6H5)2P)2CHC5H4N)2]BF4 (95936-60-0) → [RhAu(((C6H5)2P)2CHC5H4N)2](2+)*BF4(1-)*NO3(1-)=[RhAu(((C6H5)2P)2CHC5H4N)2]BF4NO3 (95936-62-2)

Guidance literature:

In dichloromethane; Rh-complex was reacted with 2 equiv. of Au-complex in CH2Cl2; Et2O was added;elem.anal.;

Reference yield: 67.0%

RhAu(C5H4NCH(P(C6H5)2)2)2(2+)*BF4(1-)*NO3(1-)=[RhAu(C5H4NCH(P(C6H5)2)2)2](BF4)(NO3) (95936-62-2) → RhAu(C5H4NCH(P(C6H5)2)2)2(CO)2(2+)*BF4(1-)*NO3(1-)=[RhAu(C5H4NCH(P(C6H5)2)2)2(CO)2](BF4)(NO3) (105473-89-0)

Guidance literature:

With CO; In dichloromethane; bubbling CO through soln. of complex (several h); N2-atmosphere; pptn. on addn. of Et2O: ppt. was filered off, washed with Et2O, and recrystd. by slow diffusion of Et2O into CH2Cl2 soln.; elem.anal.;

Reference yield: 66.0%

RhAu(C5H4NCH(P(C6H5)2)2)2(2+)*BF4(1-)*NO3(1-)=[RhAu(C5H4NCH(P(C6H5)2)2)2](BF4)(NO3) (95936-62-2) → RhAu(C5H4NCH(P(C6H5)2)2)2Cl(1+)*BF4(1-)=[RhAu(C5H4NCH(P(C6H5)2)2)2Cl]BF4 (105473-91-4)

Guidance literature:

With HCl; In dichloromethane; bubbling HCl through CH2Cl2 soln. of the complex;; immediate purging with N2; pptn. on addn. of Et2O; recrystn. (CH2Cl2/heptane, solvent diffusion); elem. anal.;

upstream raw materials:

[Rh(((C₆H₅)2P)2CHC₅H₄N)2]⁽¹⁺⁾*BF₄^(1-)=[Rh(((C₆H₅)2P)2CHC₅H₄N)2]BF₄

Downstream raw materials:

RhAu(C₅H₄NCH(P(C₆H₅)2)2)2Cl⁽¹⁺⁾*BF₄^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2Cl]BF₄

RhAu(C₅H₄NCH(P(C₆H₅)2)2)2Br⁽¹⁺⁾*BF₄^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2Br]BF₄

RhAu(C₅H₄NCH(P(C₆H₅)2)2)2(CO)2⁽²⁺⁾*BF₄^(1-)*NO₃^(1-)=[RhAu(C₅H₄NCH(P(C₆H₅)2)2)2(CO)2](BF₄)(NO₃)

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