2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate

Base Information

Chemical Name:2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate
CAS No.:1439365-46-4
Molecular Formula:C₄₅H₅₉N₇O₁₀
Molecular Weight:858.004
Hs Code.:

Synonyms:2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate

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Chemical Property of 2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate

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Technology Process of 2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate

There total 9 articles about 2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1439365-45-3
2,2’-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

: 1439365-46-4
2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate

Guidance literature:: With triethylamine; In dichloromethane; at 30 ℃;

Reference yield:

: 110126-93-7
1,4-bis((2-ethylhexyl)oxy)benzene

: 1439365-46-4
2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: nitric acid / chloroform / 1 h / 0 - 3 °C

2.1: palladium 10% on activated carbon; ammonium formate / water; isopropyl alcohol / 1 h / 80 °C / Inert atmosphere

3.1: nitrosylsulfuric acid; sulfuric acid / acetic acid; propionic acid / 0.5 h / 3 °C

3.2: Cooling with ice

4.1: nitrosylsulfuric acid; sulfuric acid / 1-methyl-pyrrolidin-2-one / 0.5 h

5.1: sodium hydrogencarbonate / dichloromethane / 40 °C

6.1: triethylamine / dichloromethane / 30 °C

With nitrosylsulfuric acid; sulfuric acid; palladium 10% on activated carbon; nitric acid; ammonium formate; sodium hydrogencarbonate; triethylamine; In 1-methyl-pyrrolidin-2-one; dichloromethane; chloroform; water; acetic acid; propionic acid; isopropyl alcohol;

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 1439365-46-4
2,2'-(4-((E)-(4-((E)-(2,4-dinitrophenyl)diazenyl)-2,5-bis(2-ethylhexyloxy)phenyl)diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) diacrylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / 18 h / Reflux

2.1: nitric acid / chloroform / 1 h / 0 - 3 °C

3.1: palladium 10% on activated carbon; ammonium formate / water; isopropyl alcohol / 1 h / 80 °C / Inert atmosphere

4.1: nitrosylsulfuric acid; sulfuric acid / acetic acid; propionic acid / 0.5 h / 3 °C

4.2: Cooling with ice

5.1: nitrosylsulfuric acid; sulfuric acid / 1-methyl-pyrrolidin-2-one / 0.5 h

6.1: sodium hydrogencarbonate / dichloromethane / 40 °C

7.1: triethylamine / dichloromethane / 30 °C

With nitrosylsulfuric acid; sulfuric acid; palladium 10% on activated carbon; nitric acid; ammonium formate; sodium hydrogencarbonate; triethylamine; potassium hydroxide; In 1-methyl-pyrrolidin-2-one; dichloromethane; chloroform; water; acetic acid; propionic acid; isopropyl alcohol;