[(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester

Base Information

Chemical Name:[(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester
CAS No.:1070770-84-1
Molecular Formula:C₂₈H₃₆N₂O₁₀
Molecular Weight:560.601
Hs Code.:

Synonyms:[(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester

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Chemical Property of [(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester

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Technology Process of [(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester

There total 4 articles about [(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1070770-82-9
2-(2-(2-amino-5-methylphenoxy)ethoxy)-5-methylbenzeneamine

: 96-32-2
bromoacetic acid methyl ester

: 1070770-84-1
[(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; Reflux;
DOI:10.1080/00397910802633421

Reference yield:

: 1070770-78-3
1-(2-chloro-ethoxy)-4-methyl-2-nitro-benzene

: 1070770-84-1
[(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 - 160 °C

2: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 20 °C / 2068.65 - 2327.23 Torr

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 90 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

: 1070770-80-7
4-methyl-2-(2-(4-methyl-2-nitrophenoxy)ethoxy)-1-nitrobenzene

: 1070770-84-1
[(2-{2-[2-(bis-methoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-5-methyl-phenyl)-methoxycarbonylmethyl-amino]-acetica cid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 20 °C / 2068.65 - 2327.23 Torr

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 90 °C

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;