Technology Process of C46H70O7Si2
There total 5 articles about C46H70O7Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dichloro-R-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl ruthenium; hydrogen;
In
ethanol;
at 35 - 40 ℃;
under 58505.9 Torr;
DOI:10.1073/pnas.1015270108
- Guidance literature:
-
Multi-step reaction with 5 steps
1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / -15 °C
2: (+/-)-CSA / toluene / Reflux
3: 2,6-dimethylpyridine / dichloromethane
4: lithium diisopropyl amide / tetrahydrofuran / -78 °C
5: dichloro-R-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl ruthenium; hydrogen / ethanol / 35 - 40 °C / 58505.9 Torr
With
2,6-dimethylpyridine; dichloro-R-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl ruthenium; hydrogen; acetic acid; tetramethylammonium triacetoxyborohydride; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1073/pnas.1015270108
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2,6-dimethylpyridine / dichloromethane
2: lithium diisopropyl amide / tetrahydrofuran / -78 °C
3: dichloro-R-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl ruthenium; hydrogen / ethanol / 35 - 40 °C / 58505.9 Torr
With
2,6-dimethylpyridine; dichloro-R-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl ruthenium; hydrogen; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1073/pnas.1015270108