2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose

Base Information

Chemical Name:2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose
CAS No.:869500-77-6
Molecular Formula:C₄₁H₄₀O₆
Molecular Weight:628.765
Hs Code.:

Synonyms:2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose

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Chemical Property of 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose

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Technology Process of 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose

There total 7 articles about 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: C₄₄H₄₆O₅S₂

: 869500-77-6
2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose

Guidance literature:: With [bis-(trifluoroacetoxy)iodo]benzene; In water; acetonitrile; at 20 ℃; for 0.5h;
DOI:10.1055/s-0039-1690158

Reference yield:

: C₄₁H₄₂O₆

: 869500-77-6
2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 25 ℃; for 2h; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.200801394

Reference yield:

: Trifluoro-methanesulfonate3-methyl-2-((2R,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-benzothiazol-3-ium;

: 869500-77-6
2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-aldehydo-D-glycero-L-manno-heptose

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran / 2 h / -10 °C

2: 350 mg / H₂O; HgCl₂ / acetonitrile; CH₂Cl₂ / 0.25 h / 20 °C

With water; mercury dichloride; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo051377w