3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide

Base Information

Chemical Name:3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide
CAS No.:1589489-89-3
Molecular Formula:C₇₂H₇₈N₂O₆
Molecular Weight:1067.42
Hs Code.:

3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide

Synonyms:3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide

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Chemical Property of 3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide

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Technology Process of 3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide

There total 6 articles about 3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: C₁₉H₁₈O₅

: 1589489-88-2
N,N'-bis(4-decyloxybenzyl)naphthalene-2,6-diamine

: 1589489-89-3
3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide

Guidance literature:: With dmap; In tetrahydrofuran; at 0 - 20 ℃; for 38h; Inert atmosphere;
DOI:10.1021/ja500841f

Reference yield:

: 767-00-0
4-cyanophenol

: 1589489-89-3
3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 0 - 35 °C / Inert atmosphere

3.1: copper(l) iodide; CVT-2537; potassium phosphate / dimethyl sulfoxide / 68 h / 115 °C / Schlenk technique; Inert atmosphere

4.1: dmap / tetrahydrofuran / 38 h / 0 - 20 °C / Inert atmosphere

With dmap; potassium phosphate; copper(l) iodide; lithium aluminium tetrahydride; CVT-2537; sodium hydride; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja500841f

Reference yield:

: 29147-90-8
4-decyloxybenzonitrile

: 1589489-89-3
3-(2-methoxynaphthalene-1-yl)propynoic acid N-{[4-(decyloxy)phenyl]methyl}-N-[6-(N-{[4-(decyloxy)phenyl]methyl}-3-(2-methoxynaphthalen-1-yl)prop-2-ynamido)naphthalen-2-yl]amide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 0 - 35 °C / Inert atmosphere

2: copper(l) iodide; CVT-2537; potassium phosphate / dimethyl sulfoxide / 68 h / 115 °C / Schlenk technique; Inert atmosphere

3: dmap / tetrahydrofuran / 38 h / 0 - 20 °C / Inert atmosphere

With dmap; potassium phosphate; copper(l) iodide; lithium aluminium tetrahydride; CVT-2537; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1021/ja500841f