C₄₀H₅₂N₄O₁₁S

Base Information

Chemical Name:C₄₀H₅₂N₄O₁₁S
CAS No.:1002095-52-4
Molecular Formula:C₄₀H₅₂N₄O₁₁S
Molecular Weight:796.939
Hs Code.:

C<sub>40</sub>H<sub>52</sub>N<sub>4</sub>O<sub>11</sub>S

Synonyms:C₄₀H₅₂N₄O₁₁S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₀H₅₂N₄O₁₁S

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Technology Process of C₄₀H₅₂N₄O₁₁S

There total 1 articles about C₄₀H₅₂N₄O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1002095-51-3
C₃₂H₄₆N₄O₉S

: 501-53-1,94274-21-2
benzyl chloroformate

: 1002095-52-4
C₄₀H₅₂N₄O₁₁S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1021/jo200553g

Reference yield:

: 1002095-52-4
C₄₀H₅₂N₄O₁₁S

: 1002095-39-7
C₃₅H₄₄N₄O₉S

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/ja077853c

Reference yield:

: 1002095-52-4
C₄₀H₅₂N₄O₁₁S

: 1002095-47-7
C₃₅H₃₈N₄O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 5 h / 0 - 20 °C

2.1: acetic acid / dichloromethane / 2 h / 20 °C / Molecular sieve; Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -60 °C

5.2: 0.25 h / -60 °C

5.3: 2 h / 20 °C

With lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; acetic acid; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2.1: Pictet-Spengler cyclisation / 5.1: Swern oxidation / 5.2: Swern oxidation;
DOI:10.1021/jo200553g