(5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride

Base Information

Chemical Name:(5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride
CAS No.:1613696-47-1
Molecular Formula:C₃₅H₃₁BrClNO₂P*Cl
Molecular Weight:679.42
Hs Code.:

Synonyms:(5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride

Suppliers and Price of (5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride

There total 1 articles about (5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1613694-85-1
(2-amino-5-bromobenzyl)(triphenyl)phosphonium chloride hydrochloride

: 344308-95-8
3-(3-chloro-4-methoxyphenyl)propionyl chloride

: 1613696-47-1
(5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride

Guidance literature:: In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h;
DOI:10.1021/ja412434f

Reference yield: 56.0%

: 1613696-47-1
(5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride

: 1613694-86-2
C₁₇H₁₅BrClNO

Guidance literature:: With potassium tert-butylate; In toluene; at 130 ℃; for 0.25h; Microwave irradiation;
DOI:10.1021/ja412434f

Reference yield:

: 1613696-47-1
(5-bromo-2-{[3-(3-chloro-4-methoxyphenyl)propanoyl]amino}benzyl)(triphenyl)phosphonium chloride

: 1613696-48-2
C₂₃H₂₆BrClN₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / toluene / 0.25 h / 130 °C / Microwave irradiation

2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 18 h / 80 °C

2.2: 27 h / 80 °C

With potassium tert-butylate; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja412434f