ethyl 1-(6-N-benzoyladenin-9-yl)-1,5,6,7,8-pentadeoxy-2,3-O-isopropylidene-β-D-ribo-non-5(E),7(E)-dienofuranuronate

Base Information

Chemical Name:ethyl 1-(6-N-benzoyladenin-9-yl)-1,5,6,7,8-pentadeoxy-2,3-O-isopropylidene-β-D-ribo-non-5(E),7(E)-dienofuranuronate
CAS No.:375397-12-9
Molecular Formula:C₂₆H₂₇N₅O₆
Molecular Weight:505.53
Hs Code.:

Synonyms:ethyl 1-(6-N-benzoyladenin-9-yl)-1,5,6,7,8-pentadeoxy-2,3-O-isopropylidene-β-D-ribo-non-5(E),7(E)-dienofuranuronate

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Chemical Property of ethyl 1-(6-N-benzoyladenin-9-yl)-1,5,6,7,8-pentadeoxy-2,3-O-isopropylidene-β-D-ribo-non-5(E),7(E)-dienofuranuronate

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Technology Process of ethyl 1-(6-N-benzoyladenin-9-yl)-1,5,6,7,8-pentadeoxy-2,3-O-isopropylidene-β-D-ribo-non-5(E),7(E)-dienofuranuronate

There total 2 articles about ethyl 1-(6-N-benzoyladenin-9-yl)-1,5,6,7,8-pentadeoxy-2,3-O-isopropylidene-β-D-ribo-non-5(E),7(E)-dienofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 375397-11-8
6-N-benzoyl-9-[5,6-dideoxy-2,3-O-isopropylidene-β-D-ribo-hept-5(E)-enodialdo-1,4-furanosyl]adenine

: 375397-12-9
ethyl 1-(6-N-benzoyladenin-9-yl)-1,5,6,7,8-pentadeoxy-2,3-O-isopropylidene-β-D-ribo-non-5(E),7(E)-dienofuranuronate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1021/jm020064f

Reference yield:

: 43077-06-1
6-N-benzoyl-2',3'-O-isopropylideneadenosine-5'-aldehyde

: 375397-12-9
ethyl 1-(6-N-benzoyladenin-9-yl)-1,5,6,7,8-pentadeoxy-2,3-O-isopropylidene-β-D-ribo-non-5(E),7(E)-dienofuranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: 625 mg / dimethylsulfoxide / 5 h

2: 65 percent / CH₂Cl₂ / 20 °C

In dichloromethane; dimethyl sulfoxide; 1: Wittig olefination / 2: Wittig olefination;
DOI:10.1021/jm020064f