1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane

Base Information

Chemical Name:1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane
CAS No.:307928-49-0
Molecular Formula:C₂₃H₄₂N₄
Molecular Weight:374.613
Hs Code.:

Synonyms:1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane

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Chemical Property of 1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane

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Technology Process of 1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane

There total 3 articles about 1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1-(3,5-di-tert-butyl-2-nitrobenzyl)-4,7-dimethyl-1,4,7-triazacyclononane

: 307928-49-0
1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 80 ℃; for 16h;
DOI:10.1021/ja001637l

Reference yield:

: 20444-30-8
1,5-di-tert-butyl-3-methyl-2-nitrobenzene

: 307928-49-0
1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / NBS; azobisisobutyronitrile / CCl₄ / Irradiation

2: 94 percent / KOH / toluene / 16 h / 80 °C

3: 78 percent / LiAlH₄ / tetrahydrofuran / 16 h / 80 °C

With potassium hydroxide; N-Bromosuccinimide; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; tetrachloromethane; toluene;
DOI:10.1021/ja001637l

Reference yield:

: 198197-34-1
2-bromomethyl-4,6-di-tert-butylnitrobenzene

: 307928-49-0
1-(2-amino-3,5-di-tert-butylbenzyl)-4,7-dimethyl-1,4,7-triazacyclononane

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / KOH / toluene / 16 h / 80 °C

2: 78 percent / LiAlH₄ / tetrahydrofuran / 16 h / 80 °C

With potassium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran; toluene;
DOI:10.1021/ja001637l