(c-C₆H₁₁)2SbH

Base Information

• Chemical Name: (c-C₆H₁₁)2SbH
• CAS No.: 1011-94-5
• Molecular Formula: C₁₂H₂₃Sb
• Molecular Weight: 289.065

Synonyms:(c-C₆H₁₁)2SbH

Chemical Property of (c-C₆H₁₁)2SbH

Chemical Property:

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Technology Process of (c-C₆H₁₁)2SbH

There total 2 articles about (c-C₆H₁₁)2SbH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(C6H11)2SbCl (1013-89-4) → (c-C6H11)2SbH (1011-94-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at -20°C, then warming; hydrolysis, distn. of the ether layer;

Reference yield:

(c-C6H11)3SbCl2 (1034-40-8) → (c-C6H11)2SbH (1011-94-5)

Guidance literature:

Multi-step reaction with 2 steps

2: LiAlH₄ / diethyl ether

With LiAlH₄; In diethyl ether;

Reference yield: 60.0%

(c-C6H11)2SbH (1011-94-5) + phenyllithium (591-51-5) → (c-C6H11)2SbLi * 1.5 dioxane

Guidance literature:

With 1,4-dioxane; In diethyl ether; shaking;

upstream raw materials:

(C₆H₁₁)2SbCl

(c-C₆H₁₁)3SbCl₂

Downstream raw materials:

{(c-C₆H₁₁)2Sb}2(CH₂)6

(c-C₆H₁₁)2SbLi

{(c-C₆H₁₁)2Sb}2(CH₂)5

(c-C₆H₁₁)2Sb(CH₂)4Cl

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