trifluoro-methanesulfonic acid 8-cyclopentyl-2-methylsulfanyl-7-oxo-7,8-dihydro-pyrido[2,3-d]pyrimidin-5-yl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid 8-cyclopentyl-2-methylsulfanyl-7-oxo-7,8-dihydro-pyrido[2,3-d]pyrimidin-5-yl ester
CAS No.:1192133-03-1
Molecular Formula:C₁₄H₁₄F₃N₃O₄S₂
Molecular Weight:409.41
Hs Code.:

Synonyms:trifluoro-methanesulfonic acid 8-cyclopentyl-2-methylsulfanyl-7-oxo-7,8-dihydro-pyrido[2,3-d]pyrimidin-5-yl ester

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Chemical Property of trifluoro-methanesulfonic acid 8-cyclopentyl-2-methylsulfanyl-7-oxo-7,8-dihydro-pyrido[2,3-d]pyrimidin-5-yl ester

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Technology Process of trifluoro-methanesulfonic acid 8-cyclopentyl-2-methylsulfanyl-7-oxo-7,8-dihydro-pyrido[2,3-d]pyrimidin-5-yl ester

There total 1 articles about trifluoro-methanesulfonic acid 8-cyclopentyl-2-methylsulfanyl-7-oxo-7,8-dihydro-pyrido[2,3-d]pyrimidin-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1192132-76-5
8-cyclopentyl-5-hydroxy-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one

: 17061-62-0
N,N-bis(p-methoxybenzyl)amine

: 1192133-03-1
trifluoro-methanesulfonic acid 8-cyclopentyl-2-methylsulfanyl-7-oxo-7,8-dihydro-pyrido[2,3-d]pyrimidin-5-yl ester

: 1192133-02-0
5-[bis-(4-methoxy-benzyl)-amino]-8-cyclopentyl-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one

Guidance literature:: trifluoromethylsulfonic anhydride; 8-cyclopentyl-5-hydroxy-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one; With triethylamine; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;

N,N-bis(p-methoxybenzyl)amine; In 1,1-dichloroethane; dichloromethane; at -78 - 100 ℃; Inert atmosphere; Microwave irradiation;

Reference yield: 93.3%

: 1192133-03-1
trifluoro-methanesulfonic acid 8-cyclopentyl-2-methylsulfanyl-7-oxo-7,8-dihydro-pyrido[2,3-d]pyrimidin-5-yl ester

: 536-74-3
phenylacetylene

: C₂₁H₁₉N₃OS

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; for 2h; Inert atmosphere; Reflux;