2-(4-N-CBZ-MORPHOLIN-2-YL)ACETIC ACID

Base Information

• Chemical Name: 2-(4-N-CBZ-MORPHOLIN-2-YL)ACETIC ACID
• CAS No.: 702693-24-1
• Molecular Formula: C₁₄H₁₇NO₅
• Molecular Weight: 279.293
• Mol file: 702693-24-1.mol

Synonyms:2-(4-N-CBZ-MORPHOLIN-2-YL)ACETIC ACID;2-CARBOXYMETHYL-MORPHOLINE-4-CARBOXYLIC ACID BENZYL ESTER;4-CBZ-2-CARBOXYMETHYL-MORPHOLINE

Chemical Property of 2-(4-N-CBZ-MORPHOLIN-2-YL)ACETIC ACID

Chemical Property:

• PSA: 76.07000
• LogP: 1.43660

Purity/Quality:

97% ^*data from raw suppliers

4-Cbz-2-carboxymethyl-morpholine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-N-CBZ-MORPHOLIN-2-YL)ACETIC ACID

There total 3 articles about 2-(4-N-CBZ-MORPHOLIN-2-YL)ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-ethoxycarbonylmethyl-morpholine-4-carboxylic acid benzyl ester → 2-carboxymethyl-morpholine-4-carboxylic acid benzyl ester (702693-24-1)

Guidance literature:

With potassium trimethylsilonate; In dichloromethane;

DOI:10.1016/S0960-894X(02)00880-6

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → 2-carboxymethyl-morpholine-4-carboxylic acid benzyl ester (702693-24-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: KOSiMe₃ / CH₂Cl₂

With potassium trimethylsilonate; triethylamine; In dichloromethane;

DOI:10.1016/S0960-894X(02)00880-6

Reference yield:

(±)-ethyl 2-(morpholin-2-yl)acetate (503601-25-0) → 2-carboxymethyl-morpholine-4-carboxylic acid benzyl ester (702693-24-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: KOSiMe₃ / CH₂Cl₂

With potassium trimethylsilonate; triethylamine; In dichloromethane;

DOI:10.1016/S0960-894X(02)00880-6

upstream raw materials:

benzyl chloroformate

(±)-ethyl 2-(morpholin-2-yl)acetate

Downstream raw materials:

2-(3-ethoxycarbonyl-2-oxo-propyl)-morpholine-4-carboxylic acid benzyl ester

2-(2-benzyloxycarbonylamino-3-carboxy-propyl)-morpholine-4-carboxylic acid benzyl ester

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