C₂₀H₂₂N₂O₂

Base Information

Chemical Name:C₂₀H₂₂N₂O₂
CAS No.:1413921-06-8
Molecular Formula:C₂₀H₂₂N₂O₂
Molecular Weight:322.407
Hs Code.:

C<sub>20</sub>H<sub>22</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₀H₂₂N₂O₂

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Chemical Property of C₂₀H₂₂N₂O₂

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Technology Process of C₂₀H₂₂N₂O₂

There total 4 articles about C₂₀H₂₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1413921-02-4
2-(2-isopropoxy-4-nitrophenyl)-5-(2-methyl-4-nitrophenyl)furan

: 1413921-06-8
C₂₀H₂₂N₂O₂

Guidance literature:: With 10% Pd/C; hydrogen; In ethanol; ethyl acetate; at 20 ℃; under 2585.81 Torr;
DOI:10.1016/j.bmcl.2012.06.037

Reference yield:

: 423165-35-9
1-bromo-2-isopropoxy-4-nitrobenzene

: 1413921-06-8
C₂₀H₂₂N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 24 h / 90 - 100 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene / 24 h / Inert atmosphere; Reflux

4: 10% Pd/C; hydrogen / ethanol; ethyl acetate / 20 °C / 2585.81 Torr

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 10% Pd/C; hydrogen; sodium carbonate; In 1,4-dioxane; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; toluene; 1: |Stille Cross Coupling / 3: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.06.037

Reference yield:

: 1413920-99-6
2-(2-isopropoxy-4-nitrophenyl)furan

: 1413921-06-8
C₂₀H₂₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene / 24 h / Inert atmosphere; Reflux

3: 10% Pd/C; hydrogen / ethanol; ethyl acetate / 20 °C / 2585.81 Torr

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 10% Pd/C; hydrogen; sodium carbonate; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide; toluene; 2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.06.037