3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone

Base Information

• Chemical Name: 3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone
• CAS No.: 1610693-10-1
• Molecular Formula: C₁₁H₈Cl₂O₄S
• Molecular Weight: 307.154

Synonyms:3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone

Chemical Property of 3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone

Chemical Property:

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Technology Process of 3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone

There total 3 articles about 3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3,4-dichloro-5-[(4-me thylphenyl)sulfanyl]-2(5H)-furanone → Mucochloric acid (766-40-5) + 3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone (1610693-10-1) + toluene-4-sulfonic acid (104-15-4)

Guidance literature:

With dihydrogen peroxide; In water; acetic acid; at 20 ℃; for 96h;

DOI:10.1134/S1070428014040149

Reference yield:

3,4-dichloro-5-[(4-me thylphenyl)sulfanyl]-2(5H)-furanone → Mucochloric acid (766-40-5) + di(p-tolyl) disulfide (103-19-5) + 3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone (1610693-10-1) + C11H8Cl2O3S (1628028-76-1) + toluene-4-sulfonic acid (104-15-4)

Guidance literature:

With dihydrogen peroxide; In water; acetic acid;

DOI:10.1134/S1070428014040149

Reference yield:

para-thiocresol (106-45-6) → di(p-tolyl) disulfide (103-19-5) + 3,4-dichloro-5-[(4-methyl phenyl)sulfonyl]-2(5H)-furanone (1610693-10-1) + C11H8Cl2O3S (1628028-76-1) + toluene-4-sulfonic acid (104-15-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / benzene / 80 °C

2: dihydrogen peroxide / acetic acid; water

With sulfuric acid; dihydrogen peroxide; In water; acetic acid; benzene;

DOI:10.1134/S1070428014040149

upstream raw materials:

para-thiocresol

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