ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate

Base Information

Chemical Name:ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate
CAS No.:957121-91-4
Molecular Formula:C₁₇H₂₅F₂NO₃S
Molecular Weight:361.453
Hs Code.:

Synonyms:ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate

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Chemical Property of ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate

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Technology Process of ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate

There total 2 articles about ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 898752-37-9
ethyl 5-(3,5-difluorophenyl)-5-oxovalerate

: 343338-28-3
(S)-2-methylpropane-2-sulfinamide

: 957121-91-4
ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate

Guidance literature:: ethyl 5-(3,5-difluorophenyl)-5-oxovalerate; (S)-2-methylpropane-2-sulfinamide; titanium(IV) tetraethanolate; In tetrahydrofuran; at 60 ℃; for 16h;

With sodium tetrahydroborate; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

Reference yield:

: 898752-37-9
ethyl 5-(3,5-difluorophenyl)-5-oxovalerate

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 957121-91-4
ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate

Guidance literature:: ethyl 5-(3,5-difluorophenyl)-5-oxovalerate; (R)-2-methylpropane-2-sulfinamide; With titanium(IV) tetraethanolate; In tetrahydrofuran; at 60 ℃; for 16h; Sealed vessel;

With sodium tetrahydroborate; In tetrahydrofuran; at 0 ℃; for 1h;

Reference yield:

: 957121-91-4
ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate

: 957121-92-5
(6S)-6-(3,5-difluorophenyl)-piperidin-2-one

Guidance literature:: ethyl (5S)-5-{[(S)-tert-butylsulfinyl]amino}-5-(3,5-difluorophenyl)pentanoate; With hydrogenchloride; In methanol; at 0 ℃; for 0.266667h; Sealed vessel;

With triethylamine; In methanol; at 65 ℃; for 3h;