C₂₆H₂₂ClNO₃

Base Information

Chemical Name:C₂₆H₂₂ClNO₃
CAS No.:1373220-66-6
Molecular Formula:C₂₆H₂₂ClNO₃
Molecular Weight:431.919
Hs Code.:

C<sub>26</sub>H<sub>22</sub>ClNO<sub>3</sub>

Synonyms:C₂₆H₂₂ClNO₃

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Chemical Property of C₂₆H₂₂ClNO₃

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Technology Process of C₂₆H₂₂ClNO₃

There total 7 articles about C₂₆H₂₂ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1373220-61-1
4-(allyl(4-chlorobenzyl)amino)-3-(allyloxy)-9H-xanthen-9-one

: 1373220-66-6
C₂₆H₂₂ClNO₃

Guidance literature:: In decalin; at 180 ℃; for 3h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c2ob07088j

Reference yield:

: 3722-51-8
3-hydroxyxanthen-9-one

: 1373220-66-6
C₂₆H₂₂ClNO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: nitric acid; acetic acid / 60 °C / Inert atmosphere

2.1: palladium on activated charcoal; hydrogen / tetrahydrofuran; methanol / 3 h / 25 °C

3.1: potassium carbonate / acetone / 0.33 h / 45 °C

3.2: 1 h / 45 °C

4.1: potassium carbonate / acetone / 25 °C

5.1: decalin / 3 h / 180 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; nitric acid; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; acetone; decalin;
DOI:10.1039/c2ob07088j

Reference yield:

: 69169-88-6
3-hydroxy-4-nitro-9H-xanthen-9-one

: 1373220-66-6
C₂₆H₂₂ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium on activated charcoal; hydrogen / tetrahydrofuran; methanol / 3 h / 25 °C

2.1: potassium carbonate / acetone / 0.33 h / 45 °C

2.2: 1 h / 45 °C

3.1: potassium carbonate / acetone / 25 °C

4.1: decalin / 3 h / 180 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; potassium carbonate; In tetrahydrofuran; methanol; acetone; decalin;
DOI:10.1039/c2ob07088j