benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate

Base Information

Chemical Name:benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate
CAS No.:1017575-24-4
Molecular Formula:C₁₉H₂₃N₃O₆
Molecular Weight:389.408
Hs Code.:

Synonyms:benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate

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Chemical Property of benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate

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Technology Process of benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate

There total 1 articles about benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 74124-79-1
di(succinimido) carbonate

: 1017575-24-4
benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate

Guidance literature:: C₅H₇NO₃*C₁₄H₂₀N₂O₂; With triethylamine; In acetonitrile; at 5 ℃;

di(succinimido) carbonate; In acetonitrile; at 2 - 2.5 ℃; for 0.833333h;

Reference yield: 76.0%

: 1017575-24-4
benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate

: 145574-59-0
(1S,5R)-7-oxo-2,6-diazabicyclo<3.2.0>heptane-6-sulfonic acid

: 1017575-57-3
(1S,5R)-2-((4S)-1-benzyloxycarbonylazepan-4-ylaminocarbonyl)-7-oxo-2,6-diazabicyclo[3.2.0]heptane-6-sulfonic acid

Guidance literature:: With sodium hydrogencarbonate; In water; acetonitrile; for 4h;

Reference yield: 50.0%

: 1017575-24-4
benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate

: 145574-59-0
(1S,5R)-7-oxo-2,6-diazabicyclo<3.2.0>heptane-6-sulfonic acid

: 1017576-20-3
(1S,5R)-2-((4S)-1-benzyloxycarbonylazepan-4-ylaminocarbonyl)-7-oxo-2,6-diazabicyclo[3.2.0]heptane-6-sulfonic acid, terbutylammonium salt

Guidance literature:: benzyl (4S)-4-(2,5-dioxopyrrolidin-1-yloxycarbonylamino)azepane-1-carboxylate; (1S,5R)-7-oxo-2,6-diazabicyclo<3.2.0>heptane-6-sulfonic acid; With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 10 ℃;

With water; In N,N-dimethyl-formamide; at 4.1 - 20 ℃; for 12.25h;

With tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; water; at 6 ℃; for 0.5h;