methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate

Base Information

• Chemical Name: methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate
• CAS No.: 76759-11-0
• Molecular Formula: C₂₂H₃₆O₃
• Molecular Weight: 348.526

Synonyms:methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate

Chemical Property of methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate

Chemical Property:

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Technology Process of methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate

There total 4 articles about methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-methyl-13-(2-methyl-4-oxo-2-cyclohexenyl)-trans,trans-6,10-tridecadien-2-yne ethylene thioketal (42722-78-1,42723-41-1,74712-41-7) → methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate (76759-11-0) + 5β-androstan-17-one (963-74-6,1912-61-4,10062-32-5,22430-34-8,34523-66-5,36378-49-1,74743-13-8)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00391a017

Reference yield:

7-methyl-13-(2-methyl-4-hydroxy-2-cyclohexenyl)-trans,trans-6,10-tridecadien-2-yne (42723-49-9) → methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate (76759-11-0) + 5β-androstan-17-one (963-74-6,1912-61-4,10062-32-5,22430-34-8,34523-66-5,36378-49-1,74743-13-8)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00391a017

Reference yield:

7-methyl-13-(2-methyl-4-oxo-2-cyclohexenyl)-trans,trans-6,10-tridecadien-2-yne ethylene thioketal (42722-78-1,42723-41-1,74712-41-7) + dimethylsulfide (75-18-3) → methyl cis,anti,trans,anti,trans-3-(2-acetyl-2,4b-dimethyl-1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydro-1-phenanthryl)propionate (76759-11-0) + 5β-androstan-17-one (963-74-6,1912-61-4,10062-32-5,22430-34-8,34523-66-5,36378-49-1,74743-13-8)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00391a017

upstream raw materials:

7-methyl-13-(2-methyl-4-oxo-2-cyclohexenyl)-trans,trans-6,10-tridecadien-2-yne ethylene thioketal

dimethylsulfide

7-methyl-13-(2-methyl-4-hydroxy-2-cyclohexenyl)-trans,trans-6,10-tridecadien-2-yne

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