1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene

Base Information

Chemical Name:1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene
CAS No.:1384173-52-7
Molecular Formula:C₃₀H₅₂O₅Si₂
Molecular Weight:548.911
Hs Code.:

Synonyms:1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene

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Chemical Property of 1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene

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Technology Process of 1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene

There total 5 articles about 1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 842132-50-7
1,5-anhydro-2-deoxy-4,6-O-di-(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolylboronic acid pinacol ester

: 1384173-52-7
1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In 1,2-dimethoxyethane; water; for 4h; Reflux;
DOI:10.1016/j.tet.2012.05.035

Reference yield:

: 1067224-53-6
C₂₃H₄₇BO₆Si₂

: 1384173-52-7
1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; water / 4 h / Reflux

With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In 1,2-dimethoxyethane; water; toluene;
DOI:10.1016/j.tet.2012.05.035

Reference yield:

: 13265-84-4
D-glucal

: 1384173-52-7
1-(1,5-anhydro-2-deoxy-4,6-O-di(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide

2.1: tert.-butyl lithium / tetrahydrofuran / -78 - 0 °C

2.2: -78 - 20 °C

3.1: toluene / 20 °C

4.1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; water / 4 h / Reflux

With 1H-imidazole; bis-triphenylphosphine-palladium(II) chloride; tert.-butyl lithium; sodium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2012.05.035