2-phenylquinolinium perchlorate

Base Information

Chemical Name:2-phenylquinolinium perchlorate
CAS No.:98847-86-0
Molecular Formula:C₁₅H₁₁N*ClHO₄
Molecular Weight:305.718
Hs Code.:

Synonyms:2-phenylquinolinium perchlorate

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Chemical Property of 2-phenylquinolinium perchlorate

Chemical Property:

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Technology Process of 2-phenylquinolinium perchlorate

There total 2 articles about 2-phenylquinolinium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 36072-73-8
1-(benzoyl)-2-phenyl-1,2-dihydroquinoline

: 98847-86-0
2-phenylquinolinium perchlorate

Guidance literature:: With 4-acetylamino-2,2,6,6-tetramethyl-piperidine-1-oxoam-monium perchlorate; In acetonitrile; at 50 ℃; for 5h;
DOI:10.1007/BF00515069

Reference yield:

: 40624-66-6
2-phenyl-1,2-dihydroquinoline

: 98847-86-0
2-phenylquinolinium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / triethylamine / diethyl ether / 3 h / Ambient temperature

2: 80 percent / 2,2,6,6-tetramethyl-1-oxopiperidinium perchlorate / acetonitrile / 5 h / 50 °C

With 4-acetylamino-2,2,6,6-tetramethyl-piperidine-1-oxoam-monium perchlorate; triethylamine; In diethyl ether; acetonitrile;
DOI:10.1007/BF00515069