N-(tert-butoxycarbonyl)-L-phenylalanine (3'R)-2'-hydroxy-tetrahydrofuran-3'-yl ester

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-L-phenylalanine (3'R)-2'-hydroxy-tetrahydrofuran-3'-yl ester
CAS No.:1262029-86-6
Molecular Formula:C₁₈H₂₅NO₆
Molecular Weight:351.4
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-L-phenylalanine (3'R)-2'-hydroxy-tetrahydrofuran-3'-yl ester

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Chemical Property of N-(tert-butoxycarbonyl)-L-phenylalanine (3'R)-2'-hydroxy-tetrahydrofuran-3'-yl ester

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Technology Process of N-(tert-butoxycarbonyl)-L-phenylalanine (3'R)-2'-hydroxy-tetrahydrofuran-3'-yl ester

There total 2 articles about N-(tert-butoxycarbonyl)-L-phenylalanine (3'R)-2'-hydroxy-tetrahydrofuran-3'-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1262029-79-7
N-(tert-butoxycarbonyl)-L-phenylalanine (2'S,3'R)-2'-acetoxy-tetrahydrofuran-3'-yl ester

: 1262029-86-6
N-(tert-butoxycarbonyl)-L-phenylalanine (3'R)-2'-hydroxy-tetrahydrofuran-3'-yl ester

Guidance literature:: With Candida antarctica lipase B; In water; acetonitrile; at 20 ℃; for 260h; regioselective reaction; Enzymatic reaction;
DOI:10.1016/j.molcatb.2010.09.008

Reference yield:

: 1262029-73-1
N-(tert-butoxycarbonyl)-L-phenylalanine 2'-hydroxy-tetrahydrofuran-3'-yl ester

: 1262029-86-6
N-(tert-butoxycarbonyl)-L-phenylalanine (3'R)-2'-hydroxy-tetrahydrofuran-3'-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Candida antarctica lipase B / chloroform / 260 h / 20 °C / Enzymatic reaction

2: Candida antarctica lipase B / water; acetonitrile / 260 h / 20 °C / Enzymatic reaction

With Candida antarctica lipase B; In chloroform; water; acetonitrile;
DOI:10.1016/j.molcatb.2010.09.008