N-(2-((1R,2R,4S)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptan-2-yl)ethyl)-2,4-dinitrobenzenesulfonamide

Base Information

Chemical Name:N-(2-((1R,2R,4S)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptan-2-yl)ethyl)-2,4-dinitrobenzenesulfonamide
CAS No.:1602487-72-8
Molecular Formula:C₁₈H₂₅N₃O₇S
Molecular Weight:427.478
Hs Code.:

Synonyms:N-(2-((1R,2R,4S)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptan-2-yl)ethyl)-2,4-dinitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-((1R,2R,4S)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptan-2-yl)ethyl)-2,4-dinitrobenzenesulfonamide

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Technology Process of N-(2-((1R,2R,4S)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptan-2-yl)ethyl)-2,4-dinitrobenzenesulfonamide

There total 2 articles about N-(2-((1R,2R,4S)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptan-2-yl)ethyl)-2,4-dinitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1656-44-6
2,4-dinitrobenzenesulfonyl chloride

: 366014-01-9
(1R,2R)-2-(2-aminoethyl)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptane

: 1602487-72-8
N-(2-((1R,2R,4S)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptan-2-yl)ethyl)-2,4-dinitrobenzenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2014.03.025

Reference yield:

: 7787-20-4,126-21-6
(1R)-fenchone

: 1602487-72-8
N-(2-((1R,2R,4S)-2-hydroxy-1,3,3-trimethylbicyclo[2.2.1]heptan-2-yl)ethyl)-2,4-dinitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -85 °C / Inert atmosphere

1.2: 1 h / -85 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether

3.1: triethylamine / dichloromethane / 24 h / 0 - 20 °C

With lithium aluminium tetrahydride; n-butyllithium; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1016/j.ejmech.2014.03.025