1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime

Base Information

Chemical Name:1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime
CAS No.:1139830-95-7
Molecular Formula:C₂₃H₂₅F₃N₄O₂
Molecular Weight:446.472
Hs Code.:

Synonyms:1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime

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Chemical Property of 1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime

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Technology Process of 1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime

There total 1 articles about 1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1139831-06-3
C₂₃H₂₄F₃N₃O₂

: 1139830-95-7
1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; sodium acetate; In ethanol; for 15h; Reflux;
DOI:10.1016/j.bmc.2008.12.034

Reference yield: 35.0%

: 1139830-95-7
1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime

: 28269-50-3
2-vinylbenzoic acid chloride

: 1139830-57-1
C₃₂H₂₉F₃N₄O₂

Guidance literature:: With 4-methyl-morpholine; In N,N-dimethyl-formamide; at 20 - 100 ℃; Microwave irradiation;
DOI:10.1016/j.bmc.2008.12.034

Reference yield: 32.0%

: 1139830-95-7
1-(5-(7-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydropyrazol-1-yl)propan-1-one oxime

: 72482-64-5
2,4-difluorobenzoyl chloride

: 1139830-51-5
2-(1-(2-(2,4-difluorophenyl)-5-methyloxazol-4-yl)-3-(2-(trifluoromethyl)phenyl)-4,5-dihydro-1H-pyrazol-5-yl)-7-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With 4-methyl-morpholine; In N,N-dimethyl-formamide; at 20 - 100 ℃; Microwave irradiation;
DOI:10.1016/j.bmc.2008.12.034