C₄₀H₅₈O₁₁

Base Information

Chemical Name:C₄₀H₅₈O₁₁
CAS No.:1373516-90-5
Molecular Formula:C₄₀H₅₈O₁₁
Molecular Weight:714.894
Hs Code.:

C<sub>40</sub>H<sub>58</sub>O<sub>11</sub>

Synonyms:C₄₀H₅₈O₁₁

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Chemical Property of C₄₀H₅₈O₁₁

Chemical Property:

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Technology Process of C₄₀H₅₈O₁₁

There total 14 articles about C₄₀H₅₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1373517-02-2
C₄₀H₆₀O₁₁

: 1373516-90-5
C₄₀H₅₈O₁₁

: 1373517-03-3
C₄₀H₅₈O₁₁

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;
DOI:10.1021/ja300565t

Reference yield:

: 1021700-94-6
C₁₉H₂₈O₅Si

: 1373516-90-5
C₄₀H₅₈O₁₁

: 1373517-03-3
C₄₀H₅₈O₁₁

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

1.2: 2 h / 0 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

3.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; sodium carbonate / toluene / 10 h / 100 °C

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / benzene / 16 h / 60 °C / Inert atmosphere

5.1: palladium on activated charcoal; hydrogen / tetrahydrofuran; ethanol / 72 h / 20 °C

6.1: pyridinium p-toluenesulfonate / dichloromethane / 3.5 h / 20 °C

7.1: diisobutylaluminium hydride / hexane; dichloromethane / 3.17 h / -40 - 0 °C

8.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 1 h / 20 °C

9.1: potassium tert-butylate / tetrahydrofuran / 0.67 h / 0 °C

10.1: tetrahydrofuran / 2.5 h / 20 °C

11.1: caesium carbonate / water / 0.25 h / 20 °C

11.2: 10 h / 50 °C

12.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 0 - 20 °C

12.2: 2 h / 20 °C

13.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; tetrapropylammonium perruthennate; dimethylsulfide borane complex; palladium on activated charcoal; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium carbonate; caesium carbonate; 4-methylmorpholine N-oxide; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene; benzene; 1.1: Wittig reaction / 1.2: Wittig reaction;
DOI:10.1021/ja300565t

Reference yield:

: 1190598-94-7
C₂₀H₃₀O₆Si

: 1373516-90-5
C₄₀H₅₈O₁₁

: 1373517-03-3
C₄₀H₅₈O₁₁

Guidance literature:: Multi-step reaction with 14 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.58 h / -78 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

2.2: 2 h / 0 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

4.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; sodium carbonate / toluene / 10 h / 100 °C

5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / benzene / 16 h / 60 °C / Inert atmosphere

6.1: palladium on activated charcoal; hydrogen / tetrahydrofuran; ethanol / 72 h / 20 °C

7.1: pyridinium p-toluenesulfonate / dichloromethane / 3.5 h / 20 °C

8.1: diisobutylaluminium hydride / hexane; dichloromethane / 3.17 h / -40 - 0 °C

9.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 1 h / 20 °C

10.1: potassium tert-butylate / tetrahydrofuran / 0.67 h / 0 °C

11.1: tetrahydrofuran / 2.5 h / 20 °C

12.1: caesium carbonate / water / 0.25 h / 20 °C

12.2: 10 h / 50 °C

13.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 0 - 20 °C

13.2: 2 h / 20 °C

14.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; tetrapropylammonium perruthennate; dimethylsulfide borane complex; palladium on activated charcoal; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium carbonate; caesium carbonate; 4-methylmorpholine N-oxide; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene; benzene; 2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1021/ja300565t