3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

Base Information

Chemical Name:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid
CAS No.:116527-83-4
Molecular Formula:C₃₃H₃₇N₃O₄
Molecular Weight:539.674
Hs Code.:

Synonyms:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

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Chemical Property of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

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Technology Process of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

There total 7 articles about 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 116527-81-2
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonitril

: 116527-83-4
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

: 116556-62-8
7-benzyloxycarbonyl-2,10-dioxo-3-hydroxy-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8,9,10-decahydro-1,7-benzodiazacyclododecin-3-carbonsaureamid

Guidance literature:: With sodium hydroxide; water; dihydrogen peroxide; In ethanol; dichloromethane; for 15h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-79-8,116527-80-1
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol

: 116527-83-4
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

2: 60 percent / sodium hydroxide, hydrogen peroxide, water / ethanol; CH₂Cl₂ / 15 h / Ambient temperature

With sodium hydroxide; water; dihydrogen peroxide; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-78-7,116556-53-7
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-3-on

: 116527-83-4
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaureamid

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

2: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

3: 60 percent / sodium hydroxide, hydrogen peroxide, water / ethanol; CH₂Cl₂ / 15 h / Ambient temperature

With sodium hydroxide; lithium aluminium tetrahydride; water; dihydrogen peroxide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)86862-9