N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide
CAS No.:126268-92-6
Molecular Formula:C₁₃H₂₀N₄O₂S
Molecular Weight:296.393
Hs Code.:

Synonyms:N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide

Suppliers and Price of N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide

There total 4 articles about N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ((S)-2-Amino-1-dimethylcarbamoyl-ethyl)-carbamic acid benzyl ester

: 126268-92-6
N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd-C / methanol

2: BH₃-Me₂S / tetrahydrofuran / 15 h / Heating

3: ethanol / 15 h / Heating

With dimethylsulfide borane complex; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/ja00202a057

Reference yield:

: 721927-33-9
benzyl (1S)-1-{[(tert-butoxycarbonyl)amino]methyl}-2-(dimethylamino)-2-oxoethylcarbamate

: 126268-92-6
N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: CF₃COOH / 1 h / Ambient temperature

2: H₂ / 10percent Pd-C / methanol

3: BH₃-Me₂S / tetrahydrofuran / 15 h / Heating

4: ethanol / 15 h / Heating

With dimethylsulfide borane complex; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/ja00202a057

Reference yield:

: 847653-44-5
(S)-2,3-Diamino-N,N-dimethyl-propionamide

: 126268-92-6
N-[(S)-4-Dimethylaminomethyl-imidazolidin-(2E)-ylidene]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: BH₃-Me₂S / tetrahydrofuran / 15 h / Heating

2: ethanol / 15 h / Heating

With dimethylsulfide borane complex; In tetrahydrofuran; ethanol;
DOI:10.1021/ja00202a057