3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine

Base Information

Chemical Name:3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine
CAS No.:1027405-35-1
Molecular Formula:C₃₈H₃₇N₃S
Molecular Weight:567.798
Hs Code.:

3-(1H-Indol-3-yl)-N<sup>1</sup>-(2-methylsulfanyl-benzyl)-N<sup>2</sup>-trityl-propane-1,2-diamine

Synonyms:3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine

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Technology Process of 3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine

There total 6 articles about 3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-(1H-Indol-3-yl)-N¹-[1-(2-methylsulfanyl-phenyl)-meth-(Z)-ylidene]-N²-trityl-propane-1,2-diamine

: 1027405-35-1
3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; for 4h;
DOI:10.1021/jm950616c

Reference yield:

: 7022-45-9
2-(methylsulfanyl)benzaldehyde

: 1027405-35-1
3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: sodium borohydride / tetrahydrofuran; methanol / 4 h

With sodium tetrahydroborate; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/jm950616c

Reference yield:

: 76-83-5
trityl chloride

: 1027405-35-1
3-(1H-Indol-3-yl)-N¹-(2-methylsulfanyl-benzyl)-N²-trityl-propane-1,2-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / triethylamine / CH₂Cl₂ / Ambient temperature

2: 48.68 g / borane methyl sulfide complex / tetrahydrofuran / 83 °C

3: toluene

4: sodium borohydride / tetrahydrofuran; methanol / 4 h

With sodium tetrahydroborate; dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jm950616c