6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine

Base Information

Chemical Name:6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine
CAS No.:1375073-90-7
Molecular Formula:C₄₁H₄₆N₁₂O₁₆
Molecular Weight:962.887
Hs Code.:

Synonyms:6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine

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Chemical Property of 6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine

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Technology Process of 6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine

There total 1 articles about 6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1236217-66-5
C₂₁H₂₉N₉O₁₁

: 1356827-06-9
C₂₂H₁₉Cl₃N₄O₆

: 1375073-90-7
6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine

Guidance literature:: C₂₁H₂₉N₉O₁₁; C₂₂H₁₉Cl₃N₄O₆; In dichloromethane; at 20 ℃; for 0.166667h; Molecular sieve; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane; at -20 - -15 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm3012992

Reference yield:

: 1375073-90-7
6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine

: C₁₉H₃₀N₁₂O₁₀

Guidance literature:: With methylamine; In ethanol; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1021/jm3012992

Reference yield:

: 1375073-90-7
6'-(R)-methyl-5-O-(5-azido-5,6-dideoxy-2,3-O-dibenzoyl-β-D-allofuranosyl)-3′,4′,6′,6-tetra-O-acetyl-2′,1,3-triazidoparomamine

: 1375073-95-2
6′-(R)-methyl-5-O-(5-amino-5,6-dideoxy-β-D-allofuranosyl)-paromamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: methylamine / ethanol / 8 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / tetrahydrofuran; water / 0.17 h / 20 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

With methylamine; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm3012992